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MB Sample ID: SA358858
Local Sample ID: | H3 |
Subject ID: | SU003431 |
Subject Type: | Plant |
Subject Species: | Pinus koraiensis |
Taxonomy ID: | 88728 |
Select appropriate tab below to view additional metadata details:
Combined analysis:
Analysis ID | AN005422 |
---|---|
Analysis type | MS |
Chromatography type | GC |
Chromatography system | Agilent 8860 GC |
Column | Agilent HP5-MS (30m x 0.25mm, 0.25 um) |
MS Type | EI |
MS instrument type | GC/MSD |
MS instrument name | Agilent 5977B |
Ion Mode | POSITIVE |
Units | Peak area |
MS:
MS ID: | MS005148 |
Analysis ID: | AN005422 |
Instrument Name: | Agilent 5977B |
Instrument Type: | GC/MSD |
MS Type: | EI |
MS Comments: | An electron ionization system with ionization energy of 7 eV was used. Helium gas (99.999%) was used as the carrier gas at constant flow rate 1 ml/min and an injection volume of 1 ul was employed. The ion-source temperature was 230 °C. The scan interval of mass spectra was 3.1 units/s and fragments from 35 to 270 da. Afterwards, Agilent MassHunter Workstation Quantitative Analysis B.07.01 were used as analytical software. The mass spectrum of the individual peak was inspected manually to confirm the peak had the correct m/z diagnostic fragments, matched with the search results from NIST MS Search 2.2 library. For endo-borneol, the target ion is m/z 95, and qualifier ions are m/z 110 and m/z 67. |
Ion Mode: | POSITIVE |