Metabolomics Workbench : NIH Data Repository

MB Sample ID: SA012762

Local Sample ID:	375
Subject ID:	SU000305
Subject Type:	Human
Subject Species:	Homo sapiens
Taxonomy ID:	9606
Age Or Age Range:	21-86
Weight Or Weight Range:	45-172 kg
Height Or Height Range:	137-200 cm
Gender:	64 M and 63 F
Human Ethnicity:	Indicated in the Study Design
Human Smoking Status:	Indicated in the Study Design
Human Alcohol Drug Use:	Indicated in the Study Design
Species Group:	Human

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Sample Preparation:

Sampleprep ID:	SP000313
Sampleprep Summary:	Each frozen serum sample was thawed and vortexed; 530 µL aliquots were mixed with 5 µL sodium azide solution (5% in H2O). The resulting solution was centrifuged, and 530 µL was transferred to a 5 mm NMR tube. A coaxial capillary containing 60 µL TSP (20.9 nmol) in D2O was placed into the NMR tube to serve as a chemical shift and quantitative reference. The samples were randomized before performing the NMR experiments.

Sampleprep ID:

SP000313

Sampleprep Summary:

Each frozen serum sample was thawed and vortexed; 530 µL aliquots were mixed with 5 µL sodium azide solution (5% in H2O). The resulting solution was centrifuged, and 530 µL was transferred to a 5 mm NMR tube. A coaxial capillary containing 60 µL TSP (20.9 nmol) in D2O was placed into the NMR tube to serve as a chemical shift and quantitative reference. The samples were randomized before performing the NMR experiments.