| Metadata details for analysis AN000921 | |
|---|---|
| Study ID | ST000601 |
| Analysis ID | AN000921 |
| Study Title | Untargeted LC-MS metabolomics analysis of human COPD plasma, HILIC & C18 |
| Institute | University of Colorado Denver |
| Species | Homo sapiens |
| Ion_mode | POSITIVE |
| MS type | ESI |
| MS Instrument Name | Agilent |
| MS Instrument Type | QTOF |
| Chromatography Instrument Name | Agilent 6520 |
| Chromatography Type | HILIC |
| Chromatography Column | Phenomenex Kinetex HILIC 100A (50 x 2.1 mm,2.6um) |
| Solvent A | 50% acetonitrile/50% water; ammonium acetate, pH 5.8 |
| Solvent B | 90% acetonitrile/10% water; pH 5.8 ammonium acetate |
| Gradient | 0.2 minutes 100% B, 2-2.1 minutes 100-90% B, 2.1-8.6 minutes 90-50% B, 8.6-8.7 minutes 50-0% B, 8.7-14.7 minutes 0% B, 14.7-14.8 minutes 0-100% B, followed by column re-equilibration |
| Flow rate | 0.6 mL/min |
| Column Temperature | 20°C |
| Retention time units | Minutes |
- UCSD Metabolomics Workbench, a resource sponsored by the Common Fund of the National Institutes of Health
|