Metadata details for analysis AN001512
Study IDST000922
Analysis IDAN001512
Study TitleCrab Urine Study
InstituteGeorgia Institute of Technology
SpeciesCallinectes sapidus
Ion_modeNEGATIVE
MS typeESI
MS Instrument NameThermo Q Exactive HF hybrid Orbitrap
MS Instrument TypeOrbitrap
Chromatography Instrument NameThermo Dionex Ultimate 3000
Chromatography TypeHILIC
Chromatography ColumnWaters Acquity BEH Amide (75 x 2.1mm,1.7um)
Solvent A100% water; 10 mM sodium acetate; 0.05% ammonium hydroxide
Solvent B100% acetonitrile; 0.05% ammonium hydroxide
Gradient(time, %A): 0, 5; 3, 63; 7, 63; 7.1, 5; 7.2, 0.5; 9.5, 5; 9.9,5.
Flow rate(time, rate (ml/min)): 0, 0.3; 3, 0.3; 7, 0.3; 7.1, 0.3; 7.2, 0.5; 9.5, 0.5; 9.9, 0.3.
Column Temperature50
Retention time unitsMinutes
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