| Metadata details for analysis AN001765 | |
|---|---|
| Study ID | ST001081 |
| Analysis ID | AN001765 |
| Study Title | Combined NMR and MS Analysis of PC patient serum (part-I) |
| Institute | Georgia Institute of Technology |
| Species | Homo sapiens |
| Ion_mode | NEGATIVE |
| MS type | ESI |
| MS Instrument Name | Thermo Q Exactive HF hybrid Orbitrap |
| MS Instrument Type | Orbitrap |
| Chromatography Instrument Name | Thermo Dionex Ultimate 3000 |
| Chromatography Type | Reversed phase |
| Chromatography Column | Waters Acquity BEH C18 (50 x 2.1mm,1.7um) |
| Solvent A | 40% water/60% acetonitrile; 0.1% formic acid; 10 mM ammonium formate |
| Solvent B | 10% acetonitrile/90% isopropanol; 0.1% formic acid; 10 mM ammonium formate |
| Gradient | 0-1 min 55% A: 1-1.1 min. 50% A; 1.1-5.0 min 45% A; 5.0-5.1 min 30% A; 5.1-8.0 min 1%A; 8.0-8.1 min 60% A; and 8.1-9.5 min held at 60% A |
| Flow rate | 400 µL min-1 |
| Column Temperature | 40 |
| Retention time units | Minutes |
- UCSD Metabolomics Workbench, a resource sponsored by the Common Fund of the National Institutes of Health
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