Metadata details for analysis AN001766
Study IDST001082
Analysis IDAN001766
Study TitleCombined NMR and MS Analysis of PC patien serum (part-II)
InstituteGeorgia Institute of Technology
SpeciesHomo sapiens
Ion_modePOSITIVE
MS typeESI
MS Instrument NameThermo Q Exactive HF hybrid Orbitrap
MS Instrument TypeOrbitrap
Chromatography Instrument NameThermo Dionex Ultimate 3000
Chromatography TypeHILIC
Chromatography ColumnWaters Xbridge BEH HILIC (75 x 2.1mm,2.5um)
Solvent A5% acetonitrile/95% water; 10 mM ammonium formate; 0.05% ammonium hydroxide
Solvent B100% acetonitrile; 0.05% ammonium hydroxide
Gradient0-7.0 min. 63% A; 7.0-7.2 min 5% A with an increased flow rate of 500 µL min-1; 7.2-9.9 min 5% A with a decreased flow rate of 300 µL min-1; and 9.9-10.0 min held at 5% A
Flow rate300 µL min-1
Column Temperature50
Retention time unitsMinutes
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