Metadata details for analysis AN002909 | |
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Study ID | ST001793 |
Analysis ID | AN002909 |
Study Title | Effect of external low-dose rate radiation on mouse biofluid metabolomic signatures (part IV) |
Institute | Georgetown University |
Species | Mus musculus |
Ion_mode | POSITIVE |
MS type | ESI |
MS Instrument Name | Waters Synapt G2 |
MS Instrument Type | QTOF |
Chromatography Instrument Name | Waters Acquity |
Chromatography Type | Reversed phase |
Chromatography Column | Waters Acquity BEH C18 (50 x 2.1mm,1.7um) |
Solvent A | 100% water; 0.1% formic acid |
Solvent B | solvent B:100% acetonitrile; 0.1% formic acid solvent C:90% isopropanol/10% acetonitrile; 0.1% formic acid |
Gradient | The gradient for urine was (solvent A and B) 4.0 min 5% B, 4.0 min 20% B, 5.1 min 95% B, and 1.9 min 5% B at a flow rate of 0.5 ml/min. The gradient for serum was (solvent A, B, and C) 4.0 min 98:2 A:B, 4.0 min 40:60 A:B, 1.5 min 2:98 A:B, 2.0 min 2:98 A:C, 0.5 min 50:50 A:C, and 1.0 min 98:2 A:B at a flow rate of 0.5 ml/min. |
Flow rate | 0.5 ml/min |
Column Temperature | |
Retention time units | Minutes |