| Metadata details for analysis AN003072 | |
|---|---|
| Study ID | ST001892 |
| Analysis ID | AN003072 |
| Study Title | Small molecule signatures of mice lacking T-cell p38 alternate activation, a model for immunosuppression conditions, after exposure to total body radiation (part II) |
| Institute | Georgetown University |
| Species | Mus musculus |
| Ion_mode | POSITIVE |
| MS type | ESI |
| MS Instrument Name | Waters Synapt G2 |
| MS Instrument Type | QTOF |
| Chromatography Instrument Name | Waters Acquity |
| Chromatography Type | Reversed phase |
| Chromatography Column | Waters Acquity BEH C18 (50 x 2.1mm,1.7um) |
| Solvent A | 100% water; 0.1% formic acid |
| Solvent B | solvent B:100% acetonitrile; 0.1% formic acid solvent C:90% isopropanol/10% acetonitrile; 0.1% formic acid |
| Gradient | The gradient for urine was (solvent A and B) 4.0 min 5% B, 4.0 min 20% B, 5.1 min 95% B, and 1.9 min 5% B at a flow rate of 0.5 ml/min. The gradient for serum was (solvent A, B, and C) 4.0 min 98:2 A:B, 4.0 min 40:60 A:B, 1.5 min 2:98 A:B, 2.0 min 2:98 A:C, 0.5 min 50:50 A:C, and 1.0 min 98:2 A:B at a flow rate of 0.5 ml/min. |
| Flow rate | 0.5 ml/min |
| Column Temperature | |
| Retention time units | Minutes |
- UCSD Metabolomics Workbench, a resource sponsored by the Common Fund of the National Institutes of Health
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