| Metadata details for analysis AN003643 | |
|---|---|
| Study ID | ST002233 |
| Analysis ID | AN003643 |
| Study Title | Batch variation of large scale LC-MS metabolomics analysis of human plasma samples |
| Institute | The Jackson Laboratory for Genomic Medicine |
| Species | Homo sapiens |
| Ion_mode | POSITIVE |
| MS type | ESI |
| MS Instrument Name | Thermo Orbitrap ID-X Tribrid |
| MS Instrument Type | Orbitrap |
| Chromatography Instrument Name | Thermo Scientific Vanquish Horizon UHPLC system |
| Chromatography Type | HILIC |
| Chromatography Column | HILIC column, AccucoreTM-150-Amide (50 x 2.1mm,2.6um) |
| Solvent A | 95% acetonitrile/5% water; 0.1% acetic acid; 10 mM ammonium acetate |
| Solvent B | 50% acetonitrile/50% water; 0.1% acetic acid; 10 mM ammonium acetate |
| Gradient | 0-0.1 min: 0% B, 0.10-5.0 min: 98% B, 5.00-5.50 min: 0% B and 4.5 min for cleaning and equilibration of column. |
| Flow rate | 0.55 ml/min |
| Column Temperature | 45 |
| Retention time units | Seconds |
- UCSD Metabolomics Workbench, a resource sponsored by the Common Fund of the National Institutes of Health
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