| Metadata details for analysis AN004202 | |
|---|---|
| Study ID | ST002552 |
| Analysis ID | AN004202 |
| Study Title | Biomarker discovery in galactosemia: Metabolomics with UPLC/HRMS in dried blood spots |
| Institute | King Saud University |
| Species | Homo sapiens |
| Ion_mode | POSITIVE |
| MS type | ESI |
| MS Instrument Name | Waters Xevo-G2-S |
| MS Instrument Type | QTOF |
| Chromatography Instrument Name | Waters Acquity |
| Chromatography Type | Reversed phase |
| Chromatography Column | Waters Acquity UPLC XSelect HSS C18 (100 × 2.1mm, 2.5um) |
| Solvent A | 100% water; 0.1% formic acid |
| Solvent B | 50% methanol/50% acetonitrile; 0.1% formic acid |
| Gradient | 0–16 min 95%–5% A, 16–19 min 5% A, 19–20 min 5%–95% A, and 20–22 min, 95%– 95% A |
| Flow rate | 300 μl/min. |
| Column Temperature | 55 |
| Retention time units | Minutes |
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