Metadata details for analysis AN004215 | |
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Study ID | ST002558 |
Analysis ID | AN004215 |
Study Title | Extraction and Untargeted Analysis of Metabolome from Undemineralised Cortical Bone Matrix for Forensic Application |
Institute | University of Central Lancashire |
Species | Homo sapiens |
Ion_mode | NEGATIVE |
MS type | ESI |
MS Instrument Name | ABI Sciex 6600 TripleTOF |
MS Instrument Type | QTOF |
Chromatography Instrument Name | Thermo Dionex Ultimate 3000 |
Chromatography Type | HILIC |
Chromatography Column | Agilent InfinityLab Poroshell 120 HILIC-Z (150 x 2.1mm,2.7um) |
Solvent A | 10 mM ammonium acetate, pH 9 with ammonium hydroxide and 10 µM medronic acid |
Solvent B | 85:15 acetonitrile / 10 mM ammonium acetate, pH 9 with ammonium hydroxide and 10 µM medronic acid in water |
Gradient | 0 min 96% B 2 min 96% B 22 min 65% B 24 min 65% B 24 min 96% B |
Flow rate | 0.25 ml/min |
Column Temperature | 50 °C |
Retention time units | Minutes |