Metadata details for analysis AN004513
Study IDST002773
Analysis IDAN004513
Study TitleA nested case-control study of untargeted plasma metabolomics and lung cancer risk among never-smoking women in Shanghai Women’s Health Study
InstituteEmory University
SpeciesHomo sapiens
Ion_modePOSITIVE
MS typeESI
MS Instrument NameThermo Q Exactive HF hybrid Orbitrap
MS Instrument TypeOrbitrap
Chromatography Instrument NameThermo Dionex Ultimate 3000 RS
Chromatography TypeHILIC
Chromatography ColumnHiggins Analytical TARGA C18 (50 x 2.1mm,5um)
Solvent A100% water
Solvent B100% acetonitrile
GradientInitial mobile phase conditions are 22.5% A, 75% B, 2.5% C hold for 1.5 min, with linear gradient to 77.5% A, 20% B, 2.5% C at 4 min, hold for 1 min, resulting in a total analytical run time of 5 min. During the flushing phase (reverse phase analytical separation), the HILIC column is equilibrated with a wash solution of 77.5% A, 20% B, 2.5% C.
Flow rate0.35-0.4 mL/min
Column Temperature40
Retention time unitsSeconds
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