Metadata details for analysis AN005181 | |
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Study ID | ST003159 |
Analysis ID | AN005181 |
Study Title | Untargeted serum metabolomics in the Parkinson's Environment and Genes (PEG) Study |
Institute | University of California, Los Angeles |
Species | Homo sapiens |
Ion_mode | POSITIVE |
MS type | ESI |
MS Instrument Name | Thermo Q Exactive HF hybrid Orbitrap |
MS Instrument Type | Orbitrap |
Chromatography Instrument Name | Thermo Dionex Ultimate 3000 |
Chromatography Type | HILIC |
Chromatography Column | Waters XBridge BEH Amide (50 x 2.1mm,2.5um) |
Solvent A | 100% water |
Solvent B | 100% acetonitrile |
Gradient | 22.5% A, 75% B, 2.5% C hold for 1.5 min, linear gradient to 77.5% A, 20% B, 2.5% C at 4 min, hold for 1 min |
Flow rate | 0.35 mL/min for 1.5 min; linear increase to 0.4 mL/min at 4 min, hold for 1 mi |
Column Temperature | 60 |
Retention time units | Seconds |