| Metadata details for analysis AN005301 | |
|---|---|
| Study ID | ST003237 |
| Analysis ID | AN005301 |
| Study Title | Plasma metabolomics of patients diagnosed with Alzheimer's Disease under Acetylcholinesterase Inhibitors treatment |
| Institute | University of Campinas |
| Species | Homo sapiens |
| Ion_mode | POSITIVE |
| MS type | ESI |
| MS Instrument Name | Thermo Q Exactive Orbitrap |
| MS Instrument Type | Orbitrap |
| Chromatography Instrument Name | Thermo Dionex Ultimate 3000 |
| Chromatography Type | Reversed phase |
| Chromatography Column | Supelco Titan C18 (1.9 μm, 2.1 x 100 mm) |
| Solvent A | 40% acetonitrile/60% water; 10 mM ammonium acetate |
| Solvent B | 10% acetonitrile/90% isopropanol;10 mM ammonium acetate |
| Gradient | The elution gradient started with 40% B from minutes 0-2, 50% B from minutes 3-6, 70% Bfrom minutes 6.1-8, 100% B from minutes 9-11, and from minutes 12-14 the column was stabilized forthe following run |
| Flow rate | 0.250 mL/min |
| Column Temperature | 45 |
| Retention time units | Minutes |
| Study ID | ST003237 |
| Analysis ID | AN005301 |
| Study Title | Plasma metabolomics of patients diagnosed with Alzheimer's Disease under Acetylcholinesterase Inhibitors treatment |
| Institute | University of Campinas |
| Species | Homo sapiens |
| Ion_mode | POSITIVE |
| MS type | ESI |
| MS Instrument Name | Thermo Q Exactive Orbitrap |
| MS Instrument Type | Orbitrap |
| Chromatography Instrument Name | Thermo Dionex Ultimate 3000 |
| Chromatography Type | Reversed phase |
| Chromatography Column | Supelco Titan C18 (1.9 μm, 2.1 x 100 mm) |
| Solvent A | 40% acetonitrile/60% water; 10 mM ammonium acetate |
| Solvent B | 10% acetonitrile/90% isopropanol;10 mM ammonium acetate |
| Gradient | The elution gradient started with 40% B from minutes 0-2, 50% B from minutes 3-6, 70% Bfrom minutes 6.1-8, 100% B from minutes 9-11, and from minutes 12-14 the column was stabilized forthe following run |
| Flow rate | 0.250 mL/min |
| Column Temperature | 45 |
| Retention time units | Minutes |