| Metadata details for analysis AN005413 | |
|---|---|
| Study ID | ST003303 |
| Analysis ID | AN005413 |
| Study Title | Metabolic Alterations in Aneurysmal Subarachnoid Hemorrhage |
| Institute | University of Akron |
| Species | Homo sapiens |
| Ion_mode | NEGATIVE |
| MS type | ESI |
| MS Instrument Name | Agilent 6545 QTOF |
| MS Instrument Type | QTOF |
| Chromatography Instrument Name | Agilent 1290 Infinity II |
| Chromatography Type | HILIC |
| Chromatography Column | HILICON iHILIC-(P) Classic HILIC column (100 x 2.1 mm, 5 µm) |
| Solvent A | 95% Water, 5% Acetonitrile; 20 mM ammonium bicarbonate; 0.1% ammonium hydroxide; 2.5 µM medronic acid |
| Solvent B | 95% Acetonitrile, 5% Water; 2.5 µM medronic acid |
| Gradient | 0-1 min: 90 % B, 1-12 min: 90-35 % B, 12-12.5 min: 35-25 % B, 12.5-14.5 min: 25 % B |
| Flow rate | 250 µL min |
| Column Temperature | 45 |
| Retention time units | Minutes |
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