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MB Sample ID: SA052569
| Local Sample ID: | PL15 |
| Subject ID: | SU000929 |
| Subject Type: | Human |
| Subject Species: | Homo sapiens |
| Taxonomy ID: | 9606 |
| Species Group: | Human |
Select appropriate tab below to view additional metadata details:
Subject:
| Subject ID: | SU000929 |
| Subject Type: | Human |
| Subject Species: | Homo sapiens |
| Taxonomy ID: | 9606 |
| Species Group: | Human |
Factors:
| Local Sample ID | MB Sample ID | Factor Level ID | Level Value | Factor Name |
|---|---|---|---|---|
| PL15 | SA052569 | FL009982 | Intact plasma | Sample type |
Collection:
| Collection ID: | CO000923 |
| Collection Summary: | Not available |
| Sample Type: | Blood |
Treatment:
| Treatment ID: | TR000943 |
| Treatment Summary: | Not available |
Sample Preparation:
| Sampleprep ID: | SP000936 |
| Sampleprep Summary: | Mixing 540 μL of urine with 60 μL D2O potassium buffer + DSS |
| Extract Storage: | -80 C |
Analysis:
| MB Sample ID: | SA052569 |
| Analysis ID: | AN001454 |
| Analysis Type: | NMR |
| Acquisition Date: | between 8/21/16 and 8/23/16 | between 8/21/16 and 8/23/17 | between 8/21/16 and 8/23/18 | between 8/21/16 and 8/23/19 | between 8/21/16 and 8/23/20 | between 8/21/16 and 8/23/21 | between 8/21/16 and 8/23/22 | between 8/21/16 and 8/23/23 |
| Acquisition Parameters File: | plasma-paper-160821/CPMG-1 plasma-paper-160822/CPMG-1 and plasma-paper-160823/CPMG-1 plasma-paper-160821/CPMG-2 plasma-paper-160822/CPMG-2 and plasma-paper-160823/CPMG-2 plasma-paper-160821/CPMG-3 plasma-paper-160822/CPMG-3 and plasma-paper-160823/CPMG-3 plasma-paper-160821/PROJECT-1 plasma-paper-160822/PROJECT-1 and plasma-paper-160826/PROJECT-1 plasma-paper-160821/NOESYPR1D plasma-paper-160822/NOESYPR1D and plasma-paper-160828/NOESYPR1D plasma-paper-160821/PURGE plasma-paper-160822/PURGE and plasma-paper-160828/PURGE plasma-paper-160821/CPMG-4 plasma-paper-160822/CPMG-4 and plasma-paper-160823/CPMG-4 plasma-paper-160821/PROJECT-2 plasma-paper-160822/PROJECT-2 and plasma-paper-160826/PROJECT-2 |
| Num Factors: | 2 |
| Num Metabolites: | 71 |
| Units: | µM |
NMR:
| NMR ID: | NM000110 |
| Analysis ID: | AN001454 |
| Instrument Name: | FT NMR |
| Instrument Type: | FT-NMR |
| NMR Experiment Type: | 1D 1H |
| NMR Comments: | For intact plasma | For intact plasma | For intact plasma | For intact plasma | For extracted plasma | For extracted plasma | For extracted plasma | For extracted plasma |
| Field Frequency Lock: | 2824.58 Hz | 2824.58 Hz | 2824.58 Hz | 2824.58 Hz | 2824.58 Hz | 2824.58 Hz | 2824.58 Hz | 2824.58 Hz |
| Spectrometer Frequency: | 600 MHz |
| NMR Solvent: | H2O+D2O (90/10) phosphate buffer | H2O+D2O (90/10) phosphate buffer | H2O+D2O (90/10) phosphate buffer | H2O+D2O (90/10) phosphate buffer | D2O phosphate buffer | D2O phosphate buffer | D2O phosphate buffer | D2O phosphate buffer |
| NMR Tube Size: | 5 mm |
| Shimming Method: | Topshim | Topshim | Topshim | Topshim | Topshim | Topshim | Topshim | Topshim Pulse Sequence | cpmgpr1d | cpmgpr1d | cpmgpr1d | PROJECTpr1d-1 | noesypr1d | zgpurge-gprefocus-2 | cpmgpr1d | PROJECTpr1d-1 |
| Water Suppression: | Presaturation |
| Pulse Width: | 19.94 μs | 19.94 μs | 19.94 μs | 19.94 μs | 11.82 μs | 11.82 μs | 11.82 μs | 11.82 μs |
| Power Level: | 5.5584 W | 5.5584 W | 5.5584 W | 5.5584 W | 5.5584 W | 5.5584 W | 5.5584 W | 5.5584 W |
| Receiver Gain: | 90.5 | 90.5 | 90.5 | 90.5 | 90.5 | 90.5 | 90.5 | 90.5 |
| Offset Frequency: | 2824.58 Hz | 2824.58 Hz | 2824.58 Hz | 2824.58 Hz | 2824.58 Hz | 2824.58 Hz | 2824.58 Hz | 2824.58 Hz |
| Presaturation Power Level: | 4.13E-05 | 4.13E-05 | 4.13E-05 | 4.13E-05 | 4.13E-05 | 4.13E-05 | 4.13E-05 | 4.13E-05 |
| Chemical Shift Ref Cpd: | DSS | DSS | DSS | DSS | DSS | DSS | DSS | DSS |
| Temperature: | 310 K | 311 K | 312 K | 313 K | 314 K | 315 K | 316 K | 317 K |
| Number Of Scans: | 32 | 32 | 32 | 32 | 32 | 32 | 32 | 32 |
| Dummy Scans: | 4 | 4 | 4 | 4 | 4 | 4 | 4 | 4 |
| Acquisition Time: | 3.067 | 3.067 | 3.067 | 3.067 | 3.067 | 3.067 | 3.067 | 3.067 |
| Relaxation Delay: | 4 s | 4 s | 4 s | 4 s | 5 s | 6 s | 7 s | 8 s |
| Spectral Width: | 20.03 ppm | 20.03 ppm | 20.03 ppm | 20.03 ppm | 20.03 ppm | 20.03 ppm | 20.03 ppm | 20.03 ppm |
| Num Data Points Acquired: | 73728 | 73728 | 73728 | 73728 | 73728 | 73728 | 73728 | 73728 |
| Real Data Points: | 36864 | 36864 | 36864 | 36864 | 36864 | 36864 | 36864 | 36864 |
| Line Broadening: | 0.3 Hz | 0.3 Hz | 0.3 Hz | 0.3 Hz | 0.3 Hz | 0.3 Hz | 0.3 Hz | 0.3 Hz |
| Zero Filling: | 65536 | 65536 | 65536 | 65536 | 65536 | 65536 | 65536 | 65536 |
| Apodization: | Gaussian | Gaussian | Gaussian | Gaussian | Gaussian | Gaussian | Gaussian | Gaussian |
| Baseline Correction Method: | Polynomial order 2 | Polynomial order 2 | Polynomial order 2 | Polynomial order 2 | Polynomial order 2 | Polynomial order 2 | Polynomial order 2 | Polynomial order 2 |
| Chemical Shift Ref Std: | DSS | DSS | DSS | DSS | DSS | DSS | DSS | DSS |
