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MB Sample ID: SA217544

Local Sample ID:Untreated_01
Subject ID:SU002353
Subject Type:Food item

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Sample Preparation:

Sampleprep ID:SP002359
Sampleprep Summary:100 µL of 1 M potassium phosphate (KH2PO4), with 0.1% sodium salt of 3-(trimethylsilyl)propionic-2,2,3,3-d4 acid (TSP-d4, chemical shift reference) in D2O were added to 900 µL of wine. The wine samples pH (originally ca. pH 3.5) was adjusted to 3.0 ± 0.03 by adding 5% (v/v) HCl in D2O, and 600 µL of the mixture were transferred into 5 mm NMR tubes.
Processing Method:None
Sample Resuspension:None
Sample Spiking:0.1% sodium salt of 3-(trimethylsilyl)propionic-2,2,3,3-d4 acid (TSP-d4), as a chemical shift reference
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