Summary of Study ST000366

This data is available at the NIH Common Fund's National Metabolomics Data Repository (NMDR) website, the Metabolomics Workbench, https://www.metabolomicsworkbench.org, where it has been assigned Project ID PR000291. The data can be accessed directly via it's Project DOI: 10.21228/M8F600 This work is supported by NIH grant, U2C- DK119886.

See: https://www.metabolomicsworkbench.org/about/howtocite.php

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Study IDST000366
Study TitleMetabolomics analysis of colon adenoma in African Americans
Study TypeMetabolomics
Study SummaryThis NMR Metabolomics analysis was performed on feces samples derived from healthy (n = 10) and adenoma (n = 10) African American subjects with the goal of identifying perturbations in metabolomics profiles in colon cancer.
Institute
University of North Carolina
DepartmentSystems and Translational Sciences
LaboratorySumner Lab
Last NameSumner
First NameSusan
AddressEastern Regional Comprehensive Metabolomics Resource Core, UNC Nutrition Research Institute, 500 Laureate Way, Kannapolis, NC, 28081
Emailsusan_sumner @unc.edu
Phone704-250-5066
Num Groups2
Total Subjects20
Raw Data AvailableYes
Raw Data File Type(s)fid
Analysis Type DetailNMR
Release Date2017-07-10
Release Version1
Susan Sumner Susan Sumner
https://dx.doi.org/10.21228/M8F600
ftp://www.metabolomicsworkbench.org/Studies/ application/zip

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NMR:

NMR ID:NM000066
Analysis ID:AN000599
Instrument Name:Bruker950 MHz
Instrument Type:Other
NMR Experiment Type:Other
NMR Comments:nmr experiment type: noesypr1d
Field Frequency Lock:Deuterium
Standard Concentration:0.5 mM
Spectrometer Frequency:950 MHz
NMR Probe:5 mm ATMA Cryoprobe
NMR Solvent:D2O
NMR Tube Size:5mm, 7 inch
Shimming Method:Topshim
Pulse Sequence:noesypr1d
Water Suppression:yes
Pulse Width:8.44 us
Power Level:12.589 W
Receiver Gain:4
Offset Frequency:4471.1 Hz
Presaturation Power Level:0.00003588 W
Chemical Shift Ref Cpd:DSS
Temperature:298.1 K
Number Of Scans:256
Dummy Scans:4
Acquisition Time:1.075 s
Relaxation Delay:2 s
Spectral Width:16 ppm, 15.243 kHz
Num Data Points Acquired:32k
Real Data Points:32k
Line Broadening:0.5 Hz
Zero Filling:yes
Apodization:Lorentzian
Baseline Correction Method:Polynomial
Chemical Shift Ref Std:DSS
Binned Increment:0.04
Binned Data Excluded Range:4.68 - 4.88 (water)
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